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Beilstein J. Org. Chem. 2014, 10, 2874–2885, doi:10.3762/bjoc.10.304
Graphical Abstract
Scheme 1: Synthesis pathway of the dimer AZO-CDim 1.
Figure 1: Overlaid UV spectra of the irradiation of AZO-CDim 1 (a) from 0 to 120 min at 365 nm and then (b) f...
Figure 2: HPLC quantification of the cis/trans ratio of AZO-CDim 1 before irradiation (left) and after irradi...
Figure 3: Percentage of cis isomer of AZO-CDim 1 produced during photoisomerization cycles (c = 10−4 M, water...
Figure 4: Representation of the most stable structures obtained for the azobenzene linker (a) for the trans c...
Figure 5: Structure of the ditopic guest ADAdim 4.
Figure 6: Titration of (a) β-CD (c = 0.8 mM) and (b) β-CD-NH2 (c = 0.8 mM) by ADAdim 4 (c = 4 mM). (c) Diluti...
Figure 7: (a) 1H NMR spectra of AZO-CDim 1 (500 MHz, D2O, 2.5 mM) in the absence (bottom) and presence of ADA...
Figure 8: Proposed structures of inclusion complexes with the ditopic host AZO-CDim 1 and the ditopic guest A...
Beilstein J. Org. Chem. 2014, 10, 2654–2657, doi:10.3762/bjoc.10.278
Figure 1: Targeted modified cyclodextrins.
Scheme 1: Synthesis of bicatenar CDs 4, 5, 6 and 7; a) succinic anhydride, 135 °C, 10 min, 70%; b) phytosphin...